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  • 1.
    Achtel, Christian
    et al.
    Friedrich Schiller University of Jena, Germany.
    Jedvert, Kerstin
    RISE - Research Institutes of Sweden, Swerea, Swerea IVF AB. Friedrich Schiller University of Jena, Germany.
    Kosan, Birgit
    Thuringian Institute of Textile and Plastics Research (TITK), Germany.
    Seoud, Omar. A.El
    University of São Paulo, Brazil.
    Heinze, Thomas
    Friedrich Schiller University of Jena, Germany.
    Dissolution capacity of novel cellulose solvents based on triethyloctylammonium chloride2017Inngår i: Macromolecular Chemistry and Physics, ISSN 1022-1352, E-ISSN 1521-3935, Vol. 218, nr 21, 1700208Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Dissolution of cellulose from various sources (microcrystalline cellulose and different dissolving grade pulp fibers) is investigated in solvent systems based on triethyl(n-octyl)ammonium chloride (N2228Cl). Clear cellulose solutions are obtained with N2228Cl in a variety of solvents, e.g., dimethyl sulfoxide, N,N-dimethylacetamide, and acetone. It is possible to prepare clear cellulose solutions from pulp fibers with concentrations up to 15 wt%. However, it is found that the cellulose is degraded, especially when neat (i.e., molten) N2228Cl is used as a solvent. The present work includes comprehensive rheological characterization of the cellulose solutions, both with shear and extensional rheology. In most cases, the viscosity values are low (complex viscosities below 100 Pa s for 5–10 wt% dissolved cellulose), and the solutions show more Newtonian than viscoelastic behavior. 

  • 2.
    Adamopoulos, Stergios
    Technological Educational Institute of Larissa, Greece.
    Fiber analysis techniques for sustainable manufacturing of corrugated board and packaging2006Inngår i: Proceedings of the 2006 Naxos International Conference on Sustainable Management and Development of Mountainous and Island Areas: 29th September - 1st October 2006, Island of Naxos, Greece / [ed] Evangelos I. Manolas, Democritus University of Thrace , 2006, Vol. 1, 1-9 s.Konferansepaper (Fagfellevurdert)
    Abstract [en]

    Environmental – economic pressure and associated regulations have led to a significant increase of recycled paper as the main fibrous component of corrugated board the last years. Corrugating packaging industry is facing the challenge to enhance products derived from recycled pulp and to ensure a satisfactory strength of packages. Advanced techniques are highly needed for the evaluation of packaging fiber supply sources as well as for the utilization of the available resources in an optimal manner. As industrial packaging is based on the characteristics of its constituent fibers, information on the fiber composition of the recycled raw materials is of primary importance for a continual control of fiber sources. This paper reports on the usefulness of fiber analysis techniques as diagnostic methods for assessing the potential quality distribution of fibers for sustainable packaging manufacturing.

  • 3.
    Adamopoulos, Stergios
    AIDIMA, Spain.
    Identification of Fibre Components in Packaging Grade Papers2006Inngår i: IAWA Journal, ISSN 0928-1541, Vol. 27, nr 2, 153-172 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Environmental and economic issues have led to a significant increase of recycled paper as the main fibrous component of corrugated board the last years. Qualitative data on the different fibre types are needed for the evaluation of packaging fibre supply sources, which are becoming numerous and heterogeneous. Fifteen different packaging grade papers (7 linerboards and 8 corrugating medium) were selected to represent all the variety of papers available on the Spanish market. The origin of virgin and recycled fibres was identified by their morphological characteristics employing light microscopy and standard fibre analysis techniques. The waste-based papers (Waste based-liners and Fluting), Kraft-liners and Test-liner were highly variable containing 9–18 different wood and nonwood components. Semi-chemical, with 5–13 components, was the less variable grade. Hardwoods were identified as the most important fibre component from a quantitative standpoint. All papers contained in their hardwood mix Betula, Eucalyptus and Populus in significant amounts. Fagus sylvatica and Tilia were also frequently observed and in some papers were amongst major hardwood components. Prominent softwood components were found to be Pinus sylvestris, P. pinaster, P. radiata, Picea, Larix and in some papers Pinus nigra. The lower presence of a variety of softwood, hardwood and nonwood (mainly grasses) species and genera was due to the paper recycling process.

  • 4.
    Adamopoulos, Stergios
    Linnéuniversitetet, Fakulteten för teknik (FTK), Institutionen för skog och träteknik (SOT).
    Morphology, properties and recyclability of modified fibres and papers with different chemicals at laboratory, pilot plant and industrial trials2015Konferansepaper (Annet (populærvitenskap, debatt, mm))
  • 5. Adamopoulos, Stergios
    Quality control of packaging fiber sources2006Konferansepaper (Annet vitenskapelig)
  • 6. Adamopoulos, Stergios
    Quantification of softwood, hardwood and nonwood fibres in packaging grade papers2006Inngår i: TAPPI Journal, ISSN 0734-1415, Vol. 5, nr 3, 27-32 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    This study determined percentages by weight of the fiber components in 15 papers commonly used to produce corrugating packaging in Spain. The papers are manufactured mainly from recycled raw materials. The percentages were determined by means of standard quantitative fiber analysis techniques and use of appropriate weight factors. Hardwoods were the major fiber component in all papers, except kraft liners, varying from 51% to 92% per weight. Kraft liners had greater softwood content (49%-69%)than hardwood, and the most plentiful softwood classes were pines. Douglas-fir was a contaminating fiber component (weight percentage less than 2%) in almost in every paper. Nonwood fibers, entering the papers through the recycling process, were a significant fiber component (2%-9%) in most of the papers, especially the waste-based papers (liners and flutings). Quantitative fiber composition reflects the differences in quality between the papers. Its usefulness could be further explored in the quality control of paper manufacturing for packaging.

    Application: Packaging grade papers incorporate a variety of wood and nonwood fiber types. Manufacturing of papers of consistent and acceptable quality requires knowledge concerning the quantity of each fiber used.

  • 7.
    Adamopoulos, Stergios
    et al.
    Linnéuniversitetet, Fakulteten för teknik (FTK), Institutionen för skog och träteknik (SOT).
    Birmpilis, D
    Technological Educational Institute of Thessaly.
    Use and properties of recovered paper raw materials for the production of corrugated board2015Inngår i: Proceedings of the 14th International Conference on Environmental Science and Technology Rhodes, Greece, 3-5 September 2015, Global NEST , 2015Konferansepaper (Fagfellevurdert)
    Abstract [en]

    The difficulty of predicting the properties of paper products produced from heterogeneous sources puts several limitations, which therefore lead to severe economic losses and only a comprehensive characterization will enable their better utilization. The project “RF-CORRUG –Quality control of raw materials from recovered fibres for the production of corrugated board”under the NationalStrategic Reference Framework 2007–2013 ARCHIMEDES IIIdeals with this common technical problem of the corrugated board industry. Specifically, the mainobjective of the project is to supportthe competitiveness of the corrugated board companies (mainly SMEs)by creatinga software tool based on practical models that can predict packaging grade paper properties from fibre data (qualitative, quantitative, morphological) used in their production. This paper presents information on the physical and mechanical properties of recovered packaging papers used in corrugated packaging. A number of different category papers (liners, flutings) used for corrugated board production in Greece were examined. The required paper properties included grammage, porosity, bursting strength, SCT, tensile strength and tearing resistance, and were measured by internationally recognized testersand standards. The data will be used to develop predictive models based on advanced statistical methods for the properties and performance of packagingaccording to information of their recovered raw paper materials.

  • 8.
    Adamopoulos, Stergios
    et al.
    Linnéuniversitetet, Fakulteten för teknik (FTK), Institutionen för skog och träteknik (SOT).
    Karageorgos, Anthony
    Technological Educational Institute of Thessaly, Greece.
    Rapti, Elli
    Center for Research and Technology – Hellas (CERTH), Greece .
    Birbilis, Dimitris
    Technological Educational Institute of Thessaly, Greece.
    Predicting the Properties of Corrugated Base Papers Using Multiple Linear Regression and  Artificial Neural Networks2016Inngår i: Drewno, ISSN 1644-3985, Vol. 59, nr 198, 61-72 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The difficulty in predicting the properties and behaviour of paper products produced using heterogeneous raw materials with high percentages of recovered fibres poses restrictions on their efficient and effective use as corrugated packaging materials. This work presents predictive models for the mechanical properties of corrugated base papers (liner and fluting-medium) from fibre and physical property data using multiple linear regression and artificial neural networks. The most significant results were obtained for the prediction of the tensile strength of liners in the cross direction from the origin (wood type, pulp method) of the fibres using linear regression, and the prediction of the compressive strength of fluting-medium in the longitudinal (machine) direction, according to the short-span test, using a neural network with one hidden layer with 6 neurons, with coefficients of determination at 95.14% and 99.28%, respectively

  • 9.
    Adamopoulos, Stergios
    et al.
    Technological Educational Institute of Larissa, Greece.
    Mai, C
    From wood fibre modification to paper technology: properties of fibres modified with DMDHEU and glutaraldehyde2011Inngår i: 3rd biennial International Fibre Engineering Conference, 24 – 26 May, Barcelona, Spain, 2011Konferansepaper (Annet vitenskapelig)
  • 10.
    Adamopoulos, Stergios
    et al.
    AIDIMA, Spain.
    Martinez, E
    AIDIMA, Spain.
    Ramirez, D.
    AIDIMA, Spain.
    Characterization of packaging grade papers from recycled raw materials through the study of fibre morphology and composition2007Inngår i: Global NEST. International Journal, ISSN 1108-4006, Vol. 9, nr 1, 20-28 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The restrictions in availability of forest-based raw materials along with favourable environmental policies towards alternative sources of raw materials have forced corrugated packaging industry to shift towards recycled paper and other fibre sources such as non-wood and agro-residues. The variability in raw pulp materials with increasing percentages of recycled fibres is a very common technical problem for the corrugated packaging industry worldwide. Corrugating packaging production is facing the challenge to ensure a satisfactory strength of packages despite the increase of recycled paper as the main fibrous component. Sustainable manufacturing of papers of consistent and acceptable quality requests comprehensive characterization of the fibrous components, which are becoming more heterogeneous. Understanding the influence that heterogeneous recycled raw materials have on packaging grade paper properties offers great potential value to the corrugated board and packaging industry.

    57 linerboards and corrugating medium were selected to represent all the variety of paper grades available on the market at the moment for the production of corrugated board in Spain. The papers were analyzed for their fibre morphology (fibre length, fibre width, lumen diameter, cell wall width and flexibility) and fibre composition (softwood to hardwood and nonwood fibre count and weight) and their strength (compression, bursting and crushing resistance) was evaluated. All the determinations were in accordance with the relevant TAPPI Test Methods. The significant differences found in most of the anatomical characteristics, fibre composition and strength properties among the paper grades reflected the diverse raw materials used for their production as well as their qualitative differences. By means of simple correlation the influence of fibre characteristics and composition on the strength of the papers was determined under two different conditions, at 23 o C and 50% RH and at 20 o C and 90% RH.

    The results demonstrate that besides the physical-mechanical characterization of packaging grade papers, fibre anatomy and composition can be used successfully as a complementary practical test to predict the performance of papers. The application of the predicting correlations is proposed for the evaluation of the fibre supplies for the packaging industry. An enormous potential for cost reduction can be created by the selection of the most appropriate and inexpensive combination of grade papers for a specific packaging use

  • 11. Adamopoulos, Stergios
    et al.
    Mertinez, E
    Ramirez, D
    Characterization of packaging grade papers from recycled raw materials through the study of fibre morphology and composition2005Inngår i: Proceedings of the 9th International Conference on Environmental Science and Technology: Rhodes, Rhodes Island, Greece, 1 - 3 September 2005 ; Volume of Abstracts / [ed] University of the Aegean, 2005, Vol. A, 18-25 s.Konferansepaper (Fagfellevurdert)
  • 12.
    Adamopoulos, Stergios
    et al.
    Technological Educational Institute of Karditsa, Greece.
    Oliver, José-Vicente
    AIDIMA, Spain.
    Fiber composition of packaging grade papers as determined by the Graff “C” staining test2006Inngår i: Wood and Fiber Science, ISSN 0735-6161, Vol. 38, nr 4, 567-575 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    A qualitative and quantitative analysis of the fiber components of 15 representative papers that are used for the production of corrugated board was carried out by the Graff "C" staining test. The method of processing of softwood, hardwood, and nonwood fibers was determined under a light microscope by their color reactions with the stain. All papers, due to the use of recycled pulp raw materials in their manufacturing, were found to incorporate in their furnish fibers that had been produced with a variety of pulping processes: chemical, mechanical, and semi-mechanical. The recycled-based papers (recycled-liner and recycled-medium) were proved to be the most variable comprising 12-15 different fiber components, while in some of the semi-chemicals only up to 7 components were identified. The weight percentages of the fiber components calculated by the application of weight factors showed that in almost all papers the most important fiber component from a quantitative standpoint was hardwood unbleached kraft followed by softwood unbleached kraft. Besides hardwood unbleached semi-chemical pulp and mechanical softwood pulp that were also plentiful in the papers, there was a smaller number of other components which sum, however, accounted for a significant fraction in the total furnish weight. The results taken on the total softwood, hardwood, and nonwood fibers content of the papers demonstrate that Graff "C" staining test is adequate to analyze both the structure and quality of packaging grade papers in practical industrial testing.

  • 13. Adamopoulos, Stergios
    et al.
    Passialis, Costas
    Voulgaridis, Elias
    Fibre characteristics of papers used in European corrugated packaging industry2009Inngår i: ATIP. Association Technique de L'Industrie Papetiere, ISSN 0997-7554, Vol. 63, nr 4, 14-21 s.Artikkel i tidsskrift (Fagfellevurdert)
  • 14. Adamopoulos, Stergios
    et al.
    Passialis, Costas
    Voulgaridis, Elias
    Fibre characteristics of papers used in European corrugated packaging industry2008Konferansepaper (Fagfellevurdert)
  • 15. Adamopoulos, Stergios
    et al.
    Passialis, Costas
    Voulgaridis, Elias
    Oliver, JV
    Utilization of recycled fibre materials in the European corrugated packaging industrial sector2008Inngår i: 2nd International Conference on Engineering for Waste Valorisation WasteEng08, June 3-5, Patras, Greece, 2008Konferansepaper (Fagfellevurdert)
  • 16. Adamopoulos, Stergios
    et al.
    Voulgaridis, E
    Passialis, C
    Morphology and identification of fibre furnish components of papers used in the production of corrugated board2013Inngår i: Celuloza Si Harti, ISSN 1220-9848Artikkel i tidsskrift (Fagfellevurdert)
  • 17.
    Adamopoulos, Stergios
    et al.
    Technological Educational Institute of Thessaly, Greece.
    Voulgaridis, Elias
    Aristotle University of Thessaloniki, Greece.
    Passialis, Costas
    Aristotle University of Thessaloniki, Greece.
    CARACTERISTICILE MATERIALULUI FIBROS ŞI PROPRIETĂŢILEHÂRTIEI RECICLATE FOLOSITE ÎN FABRICAREA CARTONULUIONDULAT: Morphology and identification of fibre furnish components of papers used in the production of corrugated board2013Inngår i: 7th International Symposium on Advanced Technologies for the Pulp, Paper and Corrugated Board Industry, 2013Konferansepaper (Fagfellevurdert)
    Abstract [ro]

    Fabricarea de ambalaje din carton ondulat (cutii, tăvi, etc) presupune un lanț de producțieintegrat, format din producătorii de hârtie, producătorii de carton ondulat și producătorii decontainere, dintre care, în Europa, majoritatea sunt IMM-uri. În prezent, containerele de cartonondulat sunt în mare parte realizate cu hârtie recuperată. Cea mai mare amenințare cu care seconfruntă lanțul de producție menționat este legat de lipsa de calitate și de disponibilitate a hârtieireciclate ca materie primă. Concret, una dintre cele mai importante proprietăți ale hârtiei deambalaj este rezistența mecanică, care depinde, în principal, de lungimea fibrelor din care estealcătuita hârtia. Aceste fibre sunt mai lungi în celuloza virgină (celuloza obţinută din lemn, adicănereciclată). Cu toate acestea, presiunea mare asupra cererii - precum și restricțiile economice șiecologice actuale referitoare la utilizarea lemnului ca materie primă - a condus la situația în caredoar o foarte mică cantitate de fibre naturale intră în lanțul de reciclare. Acest lucru înseamnă cărezistenţa fibrelor reciclate – si prin extindere – a hârtiilor – scade în mod constant, odată cuciclurile de reciclare aflate în desfăşurare. Suplimentar, hârtia reciclată prezintă o variabilitatefoarte mare, ceea ce constituie un obstacol atunci când vine vorba de a fabrica ambalaje cuproprietăţi omogene, cerute de către clienţi, la costuri fixe.Dificultatea de predicţie a proprietăților produselor din hârtie obţinute din surse eterogenepune mai multe limitări, care, din acest motiv, conduc la pierderi economice grave și numai ocaracterizare completă va permite mai buna lor folosire. Proiectul "RF-CORRUG - Controlulcalității materiilor prime din fibre recuperate pentru producția de carton ondulat", Cadrul NaționalStrategic de referinţă 2007-2013 Arhimede III, tratează această problemă tehnică comună aindustriei de carton ondulat. Concret, obiectivul principal al proiectului este de a sprijinicompetitivitatea companiilor producătoare de carton ondulat (în special IMM-uri), prin creareaunui instrument software bazat pe modele practice, care pot prezice proprietăţile sortimentului dehârtie de ambalaj, pornind de la proprietăţile fibrelor (calitative, cantitative, de structură) utilizateîn producția lor.Această lucrare prezintă informații referitoare la fibre (analiza cantitativă și calitativă,morfologia) și hârtiile de ambalaj (proprietățile fizice și mecanice) folosite în obţinereaambalajelor din carton ondulat. Au fost examinate diferite categorii de hârtii (miez şi capac),utilizate pentru producția de carton ondulat în Grecia. Principalele tehnici de analiză a fibrelor aufost: analiza masei fibroase, analiza morfologica a fibrei, microscopia optică, microscopiaelectronică de baleiaj (SEM). Suplimentar, a fost determinată rezistenţa la tracţiune (zero-spantensile test), pentru a măsura astfel rezistenţa medie a fibrei. Proprietăţile solicitate pentru hârtie au fost măsurate folosind testere şi standarderecunoscute pe plan internaţional. Informaţiile obţinute vor fi folosite pentru a dezvolta modelepredictive, bazate pe metode statistice avansate, pentru proprietăţile şi performanţele hârtiilor deambalaj, în funcţie de informaţiile furnizate de fibrele componente.

  • 18.
    Adamopoulos, Stergios
    et al.
    Greece.
    Voulgaridis, Elias
    Greece.
    Passialis, Costas
    Greece.
    Recycled Waste Paper and the Corrugated Packaging Industry in Europe2009Inngår i: Proceedings of 24th International Conference on Solid Waste Technology and Management: Philadelphia, PA USA, March 15-18, 2009, 2009, 400-411 s.Konferansepaper (Fagfellevurdert)
  • 19.
    Adamopoulos, Sterigos
    et al.
    Democritus University of Thrace, Greece.
    Oliver, José-Vicente
    AIDIMA, Spain.
    Qualitative and quantitative fibre analysis in recycled raw materials for packaging2006Inngår i: Forest products journal, ISSN 0015-7473, Vol. 56, nr 2, 58-60 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Understanding the influence that heterogeneous recycled raw materials have on packaging-grade paper performance offers great potential value to the corrugated board and packaging industry. Fifty-seven linerboards and corrugating medium were selected to represent all the variety of paper grades available on the Spanish market at the moment for the production of corrugated board. The origin of softwood, hardwood, and nonwood fibers and their percentages by weight were determined with light microscopy and standard fiber analysis techniques.

  • 20.
    Agnhage, Tove
    et al.
    Högskolan i Borås, Institutionen Textilhögskolan.
    Nierstrasz, Vincent
    Högskolan i Borås, Institutionen Textilhögskolan.
    Perwuelz, A.
    Guan, J.P.
    Chen, G.Q.
    Eco-design innovative methods for fabric finishing2014Konferansepaper (Annet vitenskapelig)
  • 21. Agnihotri, S.
    et al.
    Johnsen, I.A.
    RISE, Innventia, PFI – Paper and Fiber Research Institute.
    Moe, S.
    Gregersen, Ø.
    More selective biorefining of softwood by combined hot water and ethanol organosolv pretreatment2011Konferansepaper (Fagfellevurdert)
  • 22. Ahlberg, C.
    et al.
    Lundell, F.
    Söderberg, L. Daniel
    RISE., Innventia.
    Self-organization of fibers in a suspension between two counter-rotating discs2009Inngår i: Proceedings of the ASME Fluids Engineering Division Summer Conference 2009, 2009, Vol. 1, nr PART A, 585-592 s.Konferansepaper (Fagfellevurdert)
    Abstract [en]

    The behavior of fibers suspended in a flow between two flat counter-rotating discs has been studied experimentally. Captured images of the fibers in the flow were analyzed by steerable filters, to extract positions and orientations of the fibers. Experiments were performed for gaps between the discs of less than one fiber length, and for equal absolute values of the angular velocities for the discs. The length-to-diameter ratio of the fibers was approximately 14. During certain conditions, the fibers organized themselves in a distinct manner, which we will denote as fiber trains, in which three or more fibers are aligned next to each other, at the same radial position, with a short fiber-to-fiber distance. The direction of the individual fibers is radial and the direction of the whole train is tangential. Trains containing more than 60 fibers have been observed and are quite impressing.

  • 23.
    Ahlroth, Mikael
    et al.
    RISE - Research Institutes of Sweden, Bioekonomi.
    Bialik, Marta
    RISE - Research Institutes of Sweden, Bioekonomi.
    Jensen, Anna
    RISE - Research Institutes of Sweden, Bioekonomi.
    Hydrothermal carbonisation of effluent sludge2017Inngår i: The 7th Nordic Wood Biorefinery Conference held in Stockholm, Sweden, 28-30 Mar. 2017: NWBC 2017, Stockholm: RISE Bioekonomi , 2017, 156-158 s.Konferansepaper (Fagfellevurdert)
    Abstract [en]

    Research was carried out to investigate hydrothermal carbonisation (HTC) treatment of different effluent sludges from the pulp and paper industry in a Parr-reactor. Sludge samples were evaluated from a thermomechanical paper (TMP) mill and a kraft market pulp mill (NSWBK). The issues studied included HTC treatment time; addition of acid and alkali; dewatering properties of the resulting slurry; and non-process element (NPE) concentration in the original sludge, the filtrate and the filter cake. It was found that HTC improved the fuel quality. Alkali metals were depleted in TMP and NSWBK sludge and in both cases, the sludge was easier to dewater. The yield was better for TMP than NSWBK sludge and the yield losses had a negative impact on the NSWBK sludge. TMP sludge was already a viable boiler fuel and the treatment improved the fuel qualities even more. The HTC treatment of the NSWBK sludge resulted in lower chlorine and potassium, with lower fuel-nitrogen resulting in lower nitrous oxide. Although HTC treatment improved the low heating value of the sludge, this was counteracted by yield loss. Compared with untreated NSWBK, the overall energy impact was negative. HTC treatment offered mixed opportunities from the viewpoint of the recovery cycle.

  • 24.
    Ahmed, Sheikh Ali
    et al.
    Luleå University of Technology.
    Morén, Tom
    Luleå University of Technology.
    Hagman, Olle
    Luleå University of Technology.
    Cloutier, Alain
    Laval University, Canada.
    Fang, Chang-Hua
    Laval University, Canada.
    Elustondo, Diego
    Luleå University of Technology.
    Anatomical properties and process parameters affecting blister/blow formation in densified European aspen and downy birch sapwood boards by thermo-hygro-mechanical compression2013Inngår i: Journal of Materials Science, ISSN 0022-2461, E-ISSN 1573-4803, Vol. 48, nr 24, 8571-8579 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Approximately, 13.5 % of the standing volume of productive forest land in Sweden is covered by birch and aspen, which provides the vast potential to produce value-added products such as densified wood. This study shows whether it is possible to densify those species with a thermo-hygro-mechanical (THM) process using heat, steam, and pressure. In this process, transverse compression on thin European aspen (Populus tremula) and downy birch (Betula pubescens) boards was performed at 200 °C with a maximum steam pressure of 550 kPa. To obtain a theoretical 50 % compression set, the press’s maximum hydraulic pressure ranged from 1.5 to 7.3 MPa. Preliminary tests showed that ~75 % of the birch boards produced defects (blisters/blows) while only 25 % of the aspen boards did. Mainly, radial delamination associated with internal checks in intrawall and transwall fractures caused small cracks (termed blisters) while blows are characterized by relatively larger areas of delamination visible as a bumpy surface on the panel. Anatomical investigations revealed that birch was more prone to those defects than aspen. However, those defects could be minimized by increasing the pre-treatment time during the THM processing.

  • 25.
    Ahmed, Sheikh Ali
    et al.
    Luleå University of Technology.
    Sehlstedt-Persson, Margot
    Luleå University of Technology.
    Morén, Tom
    Luleå University of Technology.
    Development of a new rapid method for mould testing in a climate chamber: preliminary tests2013Inngår i: European Journal of Wood and Wood Products, ISSN 0018-3768, E-ISSN 1436-736X, Vol. 71, nr 4, 451-461 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The purpose of this study was to develop fast, simple and robust solid wood mould testing methods for the use in small-scale laboratory tests. The objective was to investigate mould susceptibility of different wood materials within the batches. The proposed method is based on natural contamination of non-sterile surfaces in climates conducive to mould growth. For this purpose, a climate chamber with regulated temperature and relative humidity was used. The conditioning chamber was divided into upper and lower chamber by a thin layer of stainless steel placed horizontally above the fan to minimise air circulation to the sample in the upper compartment. Mould-infected samples from outdoor tests were used as a source of mould inocula, and test trials were conducted on Scots pine (Pinus sylvestris L.) sapwood. Samples were suspended from the top of the upper chamber, and the chamber was exposed to different temperature and humidity levels. Severe mould infestation was observed after 12–14 days of incubation. Visual mould rating was then performed. Regardless of some constraints, this test method was very simple, fast, and effective. More importantly, unlike other test methods, it closely models mould infestation as it would occur under natural condition.

  • 26.
    Ahmed, Sheikh Ali
    et al.
    Luleå University of Technology.
    Sehlstedt-Persson, Margot
    Luleå University of Technology.
    Morén, Tom
    Luleå University of Technology.
    Mould susceptibility of Scots pine (Pinus sylvestris L.) sapwood: Impact of drying, thermal modification, and copper-based preservative2013Inngår i: International Biodeterioration & Biodegradation, ISSN 0964-8305, E-ISSN 1879-0208, Vol. 85, 284-288 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The development of mould on wood surfaces depends on several factors. Although mould does not affect the mechanical properties of wood, it greatly reduces the aesthetic value of wood such as the sapwood of Scots pine (Pinus sylvestris L.), which is very prone to mould. In addition, adverse health effects of mould on humans are a great concern. Different types of dried and treated wood were used to observe whether they had enhanced durability against mould following an accelerated laboratory test method in a climate chamber. Samples were green, air-dried, industrially thermally modified, treated with copper-based preservative, and kiln-dried wood, which were tested within a single test run. The test produced the following main results: The thermal modification increased the durability of the wood, and the protective effectiveness of alternative treatments was comparable to that of commercially available copper-based treatment. However, the initial moisture content of the samples during mould exposure had a great influence on the onset of mould growth. The risk of mould susceptibility of industrial kiln-dried lumber can be reduced by drying using the double-layering technique and planing off the nutrient enriched evaporation surfaces.

  • 27.
    Alberth, Lena
    KTH, Skolan för kemivetenskap (CHE).
    Experimentell studie av kinetiken vid peroxidblekning av pappersmassa2011Independent thesis Advanced level (degree of Master (Two Years)), 20 poäng / 30 hpOppgave
    Abstract [sv]

    Vid TCF-blekning av pappersmassa är väteperoxid en av huvudkemikalierna. I dagsläget är det svårt att styra blekstegen. Operatörerna måste ta hänsyn till produktionstakt, blekbarheten på massan varierar och fördröjning i trender. PO-bleksteget på Södra Cell Värö har en ungefärlig uppehållstid på 4 timmar och det är först efter så lång tid som man kan se hur en förändring verkligen slår igenom. Överblekning kostar väldigt mycket i kemikalieåtgång och det är därför efterfrågat ett sätt att kunna styra och optimera peroxidblekningssteget. Ett delsteg för detta var att simulera steget experimentellt och från dessa data ta fram en matematisk modell som förutsäger ljusheten.

    Massa togs ut från fabriken och blektes på labb under kontrollerade förhållanden med satsningar liknande verkliga i fabriken. De parametrar som studerades på labb var temperatur, väteperoxidsats och alkalisats då de påverkar ljusheten mest. En modell för ljushetsökning anpassades sedan till framtagna blekdata. Ekvationer för förbrukning av väteperoxid och hydroxidjoner togs också fram från analyser på blekfiltraten.

    Med ingående parametrar som startkoncentrationer av kemikalier, temperatur och massakoncentration förutsäger modellen ljusheten väl vid verifiering jämfört med fabrik och verifieringsblekning på labb. Modellen ligger något högre jämfört med fabrik men det var förväntat då förhållanden på labb ger ett renare system. För de parametrar som studerats anpassade sig modellen bra till förändringar och vid verifiering på labb syntes att modellen även svarade med en korrekt ljushet vid förändring i massakoncentration och ingående ljushet i steget.

  • 28. Albertsson, A.-C.
    et al.
    Voepel, J.
    Edlund, U.
    Dahlman, Olof
    RISE., Innventia.
    Söderqvist-Lindblad, M.
    Design of renewable hydrogel release systems from fiberboard mill wastewater2010Inngår i: Biomacromolecules, ISSN 1525-7797, E-ISSN 1526-4602, Vol. 11, nr 5, 1406-1411 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    A new route for the design of renewable hydrogels is presented. The soluble waste from masonite production was isolated, fractionized, and upgraded. The resulting hemicellulose rich fraction was alkenyl-functionalized and used in the preparation of covalently cross-linked hydrogels capable of sustained release of incorporated agents. Said hydrogels showed a Fickian diffusion-based release of incorporated bovine serum albumin. Also, a method for the coating of seeds with hydrogel was developed. The sustained release of incorporated growth retardant agents from the hydrogel coating on rape seeds was shown to enable the temporary inhibition of germination.

  • 29.
    Aldaeus, Fredrik
    et al.
    RISE., Innventia.
    Dedic, Dina
    RISE., Innventia.
    Karpenja, Tatjana
    RISE., Innventia.
    Magnusson, Mikael
    RISE., Innventia.
    Modorato-Rosta, Caroline
    RISE., Innventia.
    Rosén, Fredrik
    RISE., Innventia.
    Sundin, Konstantin
    RISE., Innventia.
    Lindström, Mikael
    RISE., Innventia.
    Lucisano, Marco
    RISE., Innventia.
    Towards a cellulose-based society: current trends, future scenarios, and the role of the wood biorefinery2016Inngår i: EWLP 2016. Proceedings of the 14th European workshop on lignocellulosics and pulp, Autrans 28 June - 1 July, 2016  vol. 2: Poster presentations, 2016, Vol. 2, 125-127 s.Konferansepaper (Annet vitenskapelig)
    Abstract [en]

    There is a great need to maintain research for a future in which the traditional value chains of the forest industry are combined with the needs and demands of a bio-based economy. In such a future, the pulp mill biorefinery will be a crucial node. In order to map the transformation from a fossil-based society to a cellulose-based society, a global consumer survey has been made. In addition, interviews and workshops with various players throughout the bio-economy field have been accomplished. Several current trends that affect the road to a cellulose-based society have been identified. These trends are describing the effects of urbanization, consumer behaviour, new business models, material recycling, open innovation, and the need for early demonstration of new research. The trends have been combined with uncertainties into a number of plausible scenarios describing the society and the role of cellulose in the year 2030.

  • 30.
    Aldaeus, Fredrik
    et al.
    RISE., Innventia.
    Larsson, Karolina
    RISE., Innventia.
    Stevanic Srndovic, Jasna
    RISE., Innventia.
    Kubat, Mikaela
    RISE., Innventia.
    Karlström, Katarina
    RISE., Innventia.
    Norberg, Lars
    RISE., Innventia.
    Anadolyan, Shant
    RISE., Innventia.
    Peciulyte, Ausra
    Olsson, Lisbeth
    Larsson, Per Tomas
    RISE., Innventia.
    The supramolecular structure of cellulose-rich wood and wheat straw pulps can be a determinative factor for enzymatic hydrolysability2016Inngår i: 7th Workshop on cellulose, regenerated cellulose and cellulose derivatives, Örnsköldsvik 15-16 november, 2016, 2016, 11Konferansepaper (Annet vitenskapelig)
  • 31.
    Aldaeus, Fredrik
    et al.
    RISE, Innventia.
    Larsson, Karolina
    RISE, Innventia.
    Stevanic Srndovic, Jasna
    RISE, Innventia.
    Kubat, Mikaela
    RISE, Innventia.
    Karlström, Katarina
    RISE, Innventia.
    Peciulyte, A.
    Olsson, Lars
    RISE, Innventia.
    Larsson, Per Tomas
    RISE, Innventia.
    The supramolecular structure of cellulose-rich wood pulps can be a determinative factor for enzymatic hydrolysability2015Inngår i: CelluloseArtikkel i tidsskrift (Fagfellevurdert)
  • 32.
    Aldaeus, Fredrik
    et al.
    RISE, Innventia.
    Larsson, Karolina
    RISE, Innventia.
    Stevanic Srndovic, Jasna
    RISE, Innventia.
    Kubat, Mikaela
    RISE, Innventia.
    Karlström, Katarina
    RISE, Innventia.
    Peciulyte, Ausra
    Olsson, Lisbeth
    The influence of various pulp properties on the enzymatic hydrolyzability2014Konferansepaper (Fagfellevurdert)
  • 33.
    Aldaeus, Fredrik
    et al.
    RISE., Innventia.
    Olsson, Anne-Mari
    RISE., Innventia.
    Stevanic Srndovic, Jasna
    RISE., Innventia.
    Miniaturized determination of ash content in kraft lignin samples using thermogravimetric analysis2015Inngår i: 18th International Symposium on Wood, Fiber and Pulping Chemistry, September 9-11, 2015, Vienna, 2015, 352-354 s.Konferansepaper (Annet vitenskapelig)
    Abstract [en]

    Thermogravimetric analysis (TGA) in oxidative conditions is a promising alternative to ignition in oven for the determination of inorganic residue, commonly referred to as ash. It is here shown that TGA can be used with temperature programs resembling those in standardized methods for oven ignition, and obtainequivalent results even though the sample amount is several orders of magnitude lower. The precision and limit of quantification of TGA is also discussed.

  • 34.
    Alfthan, Johan
    RISE., Innventia.
    Experimental study of non-linear stress relaxation and creep of paper materials and the relation between the two types of experiments2010Inngår i: Nordic Pulp & Paper Research Journal, ISSN 0283-2631, E-ISSN 2000-0669, Vol. 25, nr 3, 351-357 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The non-linear time-dependent mechanical behaviour of three different commercial paper grades was investigated. Stress relaxation and creep tests were carried out in MD and CD using different load levels. The strain in each test was split in a linear part and a non-linear part. From the stress and the linear part of the strain in the test, a stress relaxation modulus or a creep compliance was calculated. The stress relaxation moduli and creep compliances determined in this way were observed to be independent of the load level. The stress relaxation moduli and creep compliances for each paper were further independent of the loading direction (MD/CD) when scaled by the elastic modulus. It was also shown that the stress relaxation modulus was approximately equal to the inverse of the creep compliance, which is what would have been expected if linear viscoelastic theory had been applicable.

  • 35.
    Alfthan, Johan
    et al.
    RISE, Innventia.
    Björklund, Magnus
    Measuring creep with confidence2014Konferansepaper (Fagfellevurdert)
  • 36.
    Ali, Silvia
    et al.
    STFI-Packforsk, Stockholm, Sweden .
    Salmén, Lennart
    From wood shavings to mechanical pulp - a new raw material?2005Inngår i: Nordic Pulp & Paper Research Journal, ISSN 0283-2631, E-ISSN 2000-0669, ISSN 0283-2631, Vol. 20, nr 4, 418-422 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Wood chips used in the thermomechanical pulping (TMP) process were originally designed to suit the chemical pulping process. The production of small wood pieces more suitable for the TMP process could lead to an energy saving in this energy-intensive process. This paper discusses the potential benefits of using wood shavings instead of chips as the raw material for TMP production. In some exploratory trials, wood shavings with a thickness of about 2 mm and wood chips were refined in two steps under normal TMP process conditions in a pilot refiner. The first-stage refining was performed under pressurized conditions at 130°C. The second-stage refining was performed at atmospheric pressure at approximately 100°C at four different energy levels. The quality of the pulp produced from wood shavings was found to be better than that of the pulp produced from wood chips, with respect to both strength properties (except tear index) and optical properties at comparable energy levels. The potential for energy savings at a given tensile index using wood shavings instead of the traditional chips is estimated to be about 25%.

  • 37.
    Alimadadi, Majid
    et al.
    Mittuniversitetet, Fakulteten för naturvetenskap, teknik och medier, Avdelningen för kemiteknik.
    Uesaka, Tetsu
    Mittuniversitetet, Fakulteten för naturvetenskap, teknik och medier, Avdelningen för kemiteknik.
    3D-oriented fiber networks made by foam forming2016Inngår i: Cellulose (London), ISSN 0969-0239, E-ISSN 1572-882X, ISSN 1572-882X, Vol. 23, nr 1, 661-671 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    In industrial applications, such as paper and nonwovens, cellulose fibers are used in the form of a network where the fibers are oriented more or less in the sheet-plane direction. However, in many biological systems, fibers are instead oriented in a three-dimensional (3D) space, creating a wide variety of functionalities. In this study we created a 3D-oriented fiber network on the laboratory scale and have identified some unique features of its structure and mechanical properties. The 3D fiber network sheets were prepared by using foam-forming as well as modifying consolidation and drying procedures. The fiber orientation and tensile/compression behavior were determined. The resulting sheets were extremely bulky (above 190 cm3/g) and had extremely low stiffness (or high softness) compared to the reference handsheets. Despite this high bulk, the sheets retained good structural integrity. We found that a 3D-oriented fiber network requires much less fiber-fiber contact to create a connected (“percolated”) network than a two-dimensionally oriented network. The compression behavior in the thickness direction was also unique, characterized by extreme compressibility because of its extreme bulk and a long initial increase in the compression load as well as high strain recovery after compression because of its fiber reorientation during compression.

  • 38.
    Alimadadi, Majid
    et al.
    Mittuniversitetet, Fakulteten för naturvetenskap, teknik och medier, Avdelningen för kemiteknik.
    Uesaka, Tetsu
    Mittuniversitetet, Fakulteten för naturvetenskap, teknik och medier, Avdelningen för kemiteknik.
    Exploring One-more Dimension of Paper: Properties of 3D-Orieneted Fiber Network2014Inngår i: Progress in Paper Physics Proceedings 2014, 2014Konferansepaper (Annet vitenskapelig)
  • 39. Alm, Hajer Kamal
    et al.
    Ström, Göran
    Karlström, Katarina
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknologi.
    Schoelkopf, Joachim
    Gane, Patrick A. C.
    Effect of excess dispersant on surface properties and liquid interactions on calcium carbonate containing coatings2010Inngår i: Nordic Pulp & Paper Research Journal, ISSN 0283-2631, E-ISSN 2000-0669, Vol. 25, nr 1, 82-92 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The aim of this work was to identify what effects excess amount of sodium polyacrylate, a commonly used dispersant, has on the coating properties and the interaction between ink and the paper coating in offset printing. Since polyacrylate strongly interacts with calcium ions, soluble calcium salt was added to some coating colours to illustrate the impact of charge neutralization by calcium ions. It was found that the coating structure was only slightly affected by the extra addition of polyacrylate, showing some weak flocculation, whereas the surface chemistry was strongly influenced. The coatings became more polar and interacted more strongly with water. This resulted in slower ink setting and reduced ink-paper coating adhesion, especially in the presence of applied water/dampening solution, which are identified as contributory factors in ink piling and print mottle.

  • 40.
    Alm, H.K.
    et al.
    RISE., Innventia.
    Ström, Göran
    RISE., Innventia.
    Karlström, Katarina
    Schoelkopf, J.
    Gane, P.A.C.
    Effect of excess dispersant on surface properties and liquid interactions on calcium carbonate containing coatings2010Inngår i: Nordic Pulp & Paper Research Journal, ISSN 0283-2631, E-ISSN 2000-0669, Vol. 25, nr 1, 82-92 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The aim of this work was to identify what effects excess amount of sodium polyacrylate, a commonly used dispersant, has on the coating properties and the interaction between ink and the paper coating in offset printing. Since polyacrylate strongly interacts with calcium ions, soluble calcium salt was added to some coating colours to illustrate the impact of charge neutralization by calcium ions. It was found that the coating structure was only slightly affected by the extra addition of polyacrylate, showing some weak flocculation, whereas the surface chemistry was strongly influenced. The coatings became more polar and interacted more strongly with water. This resulted in slower ink setting and reduced ink-paper coating adhesion, especially in the presence of applied water/dampening solution, which are identified as contributory factors in ink piling and print mottle.

  • 41. Almgren, Karin
    et al.
    Gamstedt, Kristofer E.
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknik.
    Nygård, P.
    Malmberg, F.
    Lindblad, J.
    Lindström, M.
    Role of fibre-fibre and fibre-matrix adhesion in stress transfer in composites made from resin-impregnated paper sheets.2009Inngår i: International Journal of Adhesion and Adhesives, ISSN 0143-7496, E-ISSN 1879-0127, Vol. 29, nr 5, 551-557 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Paper-reinforced plastics are gaining increased interest as packaging materials, where mechanical properties are of great importance. Strength and stress transfer in paper sheets are controlled by fibre-fibre bonds. In paper-reinforced plastics, where the sheet is impregnated with a polymer resin, other stress-transfer mechanisms may be more important. The influence of fibre-fibre bonds on the strength of paper-reinforced plastics was therefore investigated. Paper sheets with different degrees of fibre-fibre bonding were manufactured and used as reinforcement in a polymeric matrix. Image analysis tools were used to verify that the difference in the degree of fibre-fibre bonding had been preserved in the composite materials. Strength and stiffness of the composites were experimentally determined and showed no correlation to the degree of fibre-fibre bonding, in contrast to the behaviour of unimpregnated paper sheets. The degree of fibre-fibre bonding is therefore believed to have little importance in this type of material, where stress is mainly transferred through the fibre-matrix interface.

  • 42.
    Almgren, Karin M.
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknik, Träkemi och massateknologi.
    Wood-fibre composites: Stress transfer and hygroexpansion2010Doktoravhandling, med artikler (Annet vitenskapelig)
    Abstract [en]

    Wood fibres is a type of natural fibres suitable for composite applications. The abundance of wood in Swedish forests makes wood-fibre composites a new and interesting application for the Swedish pulp and paper industry. For large scale production of composites reinforced by wood fibres to be realized, the mechanical properties of the materials have to be optimized. Furthermore, the negative effects of moisture, such as softening, creep and degradation, have to be limited. A better understanding of how design parameters such as choice of fibres and matrix material, fibre modifications and fibre orientation distribution affect the properties of the resulting composite material would help the development of wood-fibre composites.

    In this thesis, focus has been on the fibre-matrix interface, wood-fibre hygroexpansion and resulting mechanical properties of the composite. The importance of an efficient fibre-matrix interface for composite properties is well known, but the determination of interface properties in wood-fibre composites is difficult due to the miniscule dimensions of the fibres. This is a problem also when hygroexpansion of wood fibres is investigated. Instead of tedious single-fibre tests, more straightforward, macroscopic approaches are suggested. Halpin-Tsai’s micromechanical models and laminate analogy were used to attain efficient interface characteristics of a wood-fibre composite. When Halpin-Tsai’s model was replaced by Hashin’s concentric cylinder assembly model, a value of an interface parameter could be derived from dynamic mechanical analysis. A micromechanical model developed by Hashin was used also to identify the coefficient of hygroexpansion of wood fibres. Measurements of thickness swelling of wood-fibre composites were performed. Back-calculation through laminate analogy and the micromechanical model made it possible to estimate the wood-fibre coefficient of hygroexpansion. Through these back-calculation procedures, information of fibre and interface properties can be gained for ranking of e.g. fibre types and modifications.

    Dynamic FT-IR (Fourier Transform Infrared) spectroscopy was investigated as a tool for interface characterization at the molecular level. The effects of relative humidity in the test chamber on the IR spectra were studied. The elastic response of the matrix material increased relative to the motion of the reinforcing cellulose backbone. This could be understood as a stress transfer from fibres to matrix when moisture was introduced to the system, e.g. as a consequence of reduced interface efficiency in the moist environment. The method is still qualitative and further development is potentially very useful to measure stress redistribution on the molecular level.

  • 43.
    Almgren, Karin M.
    et al.
    Innventia.
    Gamstedt, E. Kristofer
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknik, Träkemi och massateknologi.
    Berthold, Fredrik
    Innventia.
    Lindström, Mikael
    Innventia.
    Moisture uptake and hygroexpansion of wood fiber composite materials with polylactide and polypropylene matrix materials2009Inngår i: Polymer Composites, ISSN 0272-8397, E-ISSN 1548-0569, Vol. 30, nr 12, 1809-1816 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Effects of butantetracarboxylic acid (BTCA) modification, choice of matrix, and fiber volume fraction on hygroexpansion of wood fiber composites have been investigated. Untreated reference wood fibers and BTCA-modified fibers were used as reinforcement in composites with matrices composed of polylactic acid (PLA), polypropylene (PP), or a mixture thereof. The crosslinking BTCA modification reduced the out-of-plane hygroexpansion of PLA and PLA/PP composites, under water-immersed and humid conditions, whereas the swelling increased when PP was used as matrix material. This is explained by difficulties for the BTCA-modified fibers to adhere to the PP matrix. Fiber volume fraction was the most important parameter as regards out-of-plane hygroexpansion, with a high-fiber fraction leading to large hygroexpansion. Fiber-matrix wettability during processing and consolidation also showed to have a large impact on the dimensional stability and moisture uptake. POLYM. COMPOS., 30:1809-1816, 2009.

  • 44. Almgren, Karin M.
    et al.
    Gamstedt, E. Kristofer
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknik, Träkemi och massateknologi.
    Varna, Janis
    Luleå tekniska universitet, LTU.
    Contribution of wood fiber hygroexpansion to moisture induced thickness swelling of composite plates2010Inngår i: Polymer Composites, ISSN 0272-8397, E-ISSN 1548-0569, Vol. 31, nr 5, 762-771 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    One of the main drawbacks of wood fiber-based composite materials is their propensity to swell due to moisture uptake. Because the wood fibers are usually the main contributor to hygroexpansion, it is of interest to quantify the hygroexpansion coefficient of wood fibers, to compare and rank different types of fibers. This investigation outlines an inverse method to estimate the transverse hygroexpansion coefficient of wood fibers based on measurements of moisture induced thickness swelling of composite plates. The model is based on composite micromechanics and laminate theory. Thickness swelling has been measured on polylactide matrix composites with either bleached reference fibers or crosslinked fibers. The crosslinking modification reduced the transverse hygroexpansion of the composites and the transverse coefficient of hygroexpansion of the fibers was reduced from 0.28 strain per relative humidity for reference fibers to 0.12 for cross-linked fibers

  • 45. Almgren, Karin M.
    et al.
    Åkerholm, Margaretha
    Gamstedt, Kristofer
    Salmén, Lennart
    Lindström, Mikael
    Effects of Moisture on Dynamic Mechanical Properties of Wood Fiber Composites Studied by Dynamic FT-IR Spectroscopy2008Inngår i: Journal of reinforced plastics and composites (Print), ISSN 0731-6844, E-ISSN 1530-7964, Vol. 27, nr 16-17, 1709-1721 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Wood fiber reinforced polylactide is a biodegradable composite where both fibers and matrix are from renewable resources. In the development of such new materials, information on mechanical behavior on the macroscopic and the molecular level is useful. In this study, dynamic Fourier transform infrared (FT-IR) spectroscopy is used to measure losses at the molecular level during cyclic tensile loading for bonds that are characteristic of the cellulosic fibers and the polylactid matrix. This molecular behavior is compared with measured macroscopic hysteresis losses for different moisture levels. The results show that moisture ingress will transfer the load from the fibers to the matrix, and that a more efficient fiber-matrix interface would diminish mechanical losses. Although the dynamic FT-IR spectroscopy method is still qualitative, this investigation shows that it can provide information on the stress transfer of the constituents in wood fiber reinforced plastics.

  • 46.
    Almgren, K.M.
    et al.
    RISE., Innventia.
    Gamstedt, E.K.
    RISE., Innventia.
    Characterization of interfacial stress transfer ability by dynamic mechanical analysis of cellulose fiber based composite materials2010Inngår i: Composite interfaces (Print), ISSN 0927-6440, E-ISSN 1568-5543, Vol. 17, nr 9, 845-861 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    The stress transfer ability at the fiber-matrix interface of wood fiber composites is known to affect the mechanical properties of the composite. The evaluation of interface properties at the level of individual fibers is however difficult due to the small dimensions and variability of the fibers. The dynamical mechanical properties of composite and constituents, in this case wood fibers and polylactide matrix, was here used together with micromechanical modeling to quantify the stress transfer efficiency at the fiber-matrix interface. To illustrate the methodology, a parameter quantifying the degree of imperfection at the interface was identified by inverse modeling using a micromechanical viscoelastic general self-consistent model with an imperfect interface together with laminate analogy on the composite level. The effect of moisture was assessed by comparison with experimental data from dynamic mechanical analysis in dry and moist state. For the wood fiber reinforced polylactide, the model shows that moisture absorption led to softening and mechanical dissipation in the hydrophilic wood fibers and biothermoplastic matrix, rather than loss of interfacial stress transfer ability.

  • 47.
    Almlöf Ambjörnsson, Heléne
    et al.
    Karlstads universitet, Fakulteten för teknik- och naturvetenskap, Avdelningen för kemiteknik.
    Germgård, Ulf
    Karlstads universitet, Fakulteten för teknik- och naturvetenskap, Avdelningen för kemiteknik.
    Enzyme treatment of dissolving pulps as a way to improve the following dissolution of the fibres2012Konferansepaper (Annet vitenskapelig)
  • 48. Ambjörnsson, H.A.
    et al.
    Östberg, L.
    Schenzel, K.
    Larsson, P.T.
    RISE, Innventia.
    Germgård, U.
    Enzyme pretreatment of dissolving pulp as a way to improve the following dissolution in NaOH/ZnO2014Inngår i: Holzforschung, ISSN 0018-3830, E-ISSN 1437-434X, Vol. 68, nr 4, 385-391 s.Artikkel i tidsskrift (Fagfellevurdert)
  • 49.
    Aminzadeh, Selda
    et al.
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknologi.
    Zhang, Liming
    Henriksson, Gunnar
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknologi.
    A possible explanation for the structural inhomogeneity of lignin in LCC networks2017Inngår i: Wood Science and Technology, ISSN 0043-7719, E-ISSN 1432-5225, Vol. 51, nr 6, 1365-1376 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Lignin has a very complex structure, and this is partly due to the monomers being connected by many different types of covalent bonds. Furthermore, there are multiple covalent bonds between lignin and polysaccharides in wood, and it is known that the structure of lignin covalently bound to the hemicellulose xylan is different to lignin bound to the hemicellulose glucomannan. Here, synthetic lignin (DHP) is synthesized at different pH and it is shown that lignin made at lower pH has a structure more similar to the lignin bound to xylan, i.e., having higher relative content of beta-O-4 ethers. It is hypothesized that xylan due to its carboxylic acids forms a locally lower pH and thus "direct" the lignin structure to have more beta-O-4 ethers. The biological significance of these results is discussed.

  • 50.
    Aminzadeh, Selda
    et al.
    KTH, Skolan för kemivetenskap (CHE), Fiber- och polymerteknologi. KTH, Skolan för kemivetenskap (CHE), Centra, Wallenberg Wood Science Center.
    Zhang, Liming
    Henriksson, Gunnar
    KTH, Skolan för kemivetenskap (CHE), Centra, Wallenberg Wood Science Center.
    A possible explanation for the structural inhomogeneity of lignin in LCC networks2017Inngår i: Wood Science and Technology, ISSN 0043-7719, E-ISSN 1432-5225, Vol. 51, nr 6, 1365-1376 s.Artikkel i tidsskrift (Fagfellevurdert)
    Abstract [en]

    Lignin has a very complex structure, and this is partly due to the monomers being connected by many different types of covalent bonds. Furthermore, there are multiple covalent bonds between lignin and polysaccharides in wood, and it is known that the structure of lignin covalently bound to the hemicellulose xylan is different to lignin bound to the hemicellulose glucomannan. Here, synthetic lignin (DHP) is synthesized at different pH and it is shown that lignin made at lower pH has a structure more similar to the lignin bound to xylan, i.e., having higher relative content of beta-O-4 ethers. It is hypothesized that xylan due to its carboxylic acids forms a locally lower pH and thus "direct" the lignin structure to have more beta-O-4 ethers. The biological significance of these results is discussed.

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