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  • 1.
    van der Werf, Angela
    et al.
    Stockholm University, Faculty of Science, Department of Organic Chemistry.
    Hribersek, Matic
    Stockholm University, Faculty of Science, Department of Organic Chemistry.
    Selander, Nicklas
    Stockholm University, Faculty of Science, Department of Organic Chemistry.
    N-Trifluoromethylation of Nitrosoarenes with Sodium Triflinate2017In: Organic Letters, ISSN 1523-7060, E-ISSN 1523-7052, Vol. 19, no 9, p. 2374-2377Article in journal (Refereed)
    Abstract [en]

    A highly efficient N-trifluoromethylation of nitro-soarenes is reported. The inexpensive and convenient Langlois reagent (sodium triflinate) is employed as a Ch(3)-radical source in combination with a copper catalyst and an oxidant. N-Trifluoromethylated hychoxylamines are obtained in high yields within 1 h at room temperature. The addition of hydroquinone was found to be instrumental to prevent the formation of side products. The method is high-yielding is scalable, and displays a high functional group tolerance.

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