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Heat treatments of high temperature dried norway spruce boards: Saccharides and furfurals in sapwood surfaces
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Wood Science and Engineering.ORCID iD: 0000-0002-7711-9267
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Wood Science and Engineering.ORCID iD: 0000-0002-3544-8716
Luleå University of Technology, Department of Engineering Sciences and Mathematics, Wood Science and Engineering.
2012 (English)In: BioResources, ISSN 1930-2126, E-ISSN 1930-2126, Vol. 7, no 2, 2284-2299 p.Article in journal (Refereed) Published
Abstract [en]

Carbohydrates that migrate to wood surfaces in sapwood during drying might influence properties such as mould susceptibility and colour. Sugars on the surface of Norway spruce boards during various heat treatments were studied. Samples (350mm×125mm×25mm) were double-stacked, facing sapwood-side outwards, and dried at 110°C to a target moisture content (MC) of 40%. Dried sub-samples (80 mm × 125 mm × 25 mm) were stacked in a similar way and further heated at 110°C and at 130°C for 12, 24, and 36 hours, respectively. Glucose, fructose, and sucrose as well as 5-hydroxymethylfurfural (HMF) and furfural in the sapwood surface layer of treated wood were analysed using HPLC (RI- and UV-detectors). Carbohydrates degraded to a lower extent at 110°C than at 130°C. Furfural and to a larger extent HMF increased with treatment period and temperature. Heat treatment led to a decrease in lightness and hue of the sapwood surface of sub-samples, while chroma increased somewhat. Furthermore, considerably faster degradation (within a few minutes) of the carbohydrates on the surface of the dried spruce boards was observed when single sub-samples were conductively hot pressed at 200°C. Treatment period and initial MC influenced the presence of the carbohydrates in wood surface as well as colour change (ΔE ab) of the hot pressed sub-samples.

Place, publisher, year, edition, pages
2012. Vol. 7, no 2, 2284-2299 p.
National Category
Bio Materials
Research subject
Wood Physics
Identifiers
URN: urn:nbn:se:ltu:diva-2606Local ID: 03d25798-840b-4770-aaf6-953276bf6d7dOAI: oai:DiVA.org:ltu-2606DiVA: diva2:975459
Note
Validerad; 2012; 20120807 (ysko)Available from: 2016-09-29 Created: 2016-09-29 Last updated: 2017-11-24Bibliographically approved

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