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Biaxial flexural strength and surface characterization of multilayer zirconium dioxide after polishing, glazing and clinical adjustments
Malmö University, Faculty of Odontology (OD).ORCID iD: 0000-0001-6693-8278
Malmö University, Faculty of Odontology (OD). Faculty of Dentistry, Riga Stradins University, Riga, Latvia.ORCID iD: 0000-0002-3912-0830
Malmö University, Faculty of Odontology (OD).ORCID iD: 0000-0001-6260-473X
2025 (English)In: Journal of The Mechanical Behavior of Biomedical Materials, ISSN 1751-6161, E-ISSN 1878-0180, Vol. 166, article id 106930Article in journal (Refereed) Published
Abstract [en]

PURPOSE: To evaluate how laboratory polishing and glazing and clinical adjustments, i.e., by grinding and polishing affect the biaxial flexural strength and surface characterization of multilayer zirconia.

METHODS: Specimens of KATANA™ Zirconia YML, containing Enamel-Body 1 or Body 2-3 layers, and UTML were divided into 18 groups (n = 11) according to material/layer and finish treatment: laboratory polishing, glazing, or both, or followed by clinical adjustments. The surface roughness, surface structure and elemental composition were evaluated. Thermocyclic-mechanical cyclic loading and biaxial flexural strength test were performed. Three- and two-way ANOVA were used (α = 0.05).

RESULTS: The yttrium amount decreased in the order UTML, YML Enamel-Body 1, and YML Body 2-3. Body 2-3 showed higher flexural strength than Enamel-Body 1 and UTML, in that order. Flexural strength after clinical adjustments was higher in Body 2-3 but lower in Enamel-Body 1 and UTML. Finish treatments had indistinguishable impact on Enamel-Body 1. Body 2-3 had higher strength after polishing, polishing and glazing, and glazing, in that order. UTML displayed the highest strength after polishing and glazing or glazing. The surface roughness was lowest after polishing regardless of material/layer.

CONCLUSIONS: Laboratory treatments and clinical adjustments of multilayer zirconia affect the flexural strength and surface roughness differently depending on the zirconia type. Composition-gradient zirconia should be polished, and shade-gradient zirconia (≥ 5 mol% yttria) should be polished and glazed. Clinical adjustments of zirconia with higher yttria content are detrimental for the flexural strength and should be performed with caution.

Place, publisher, year, edition, pages
Elsevier, 2025. Vol. 166, article id 106930
Keywords [en]
Elemental composition, Grinding, Microstructure, Strength-gradient, Surface finish treatment, Surface roughness, YSZ
National Category
Odontology
Identifiers
URN: urn:nbn:se:mau:diva-74306DOI: 10.1016/j.jmbbm.2025.106930ISI: 001432447900001PubMedID: 39987645Scopus ID: 2-s2.0-85218269074OAI: oai:DiVA.org:mau-74306DiVA, id: diva2:1939695
Available from: 2025-02-24 Created: 2025-02-24 Last updated: 2025-03-19Bibliographically approved

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