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A laboratory-based double X-ray spectrometer for simultaneous X-ray emission and X-ray absorption studies
Polish Acad Sci, Inst Phys Chem, 44-52 Kasprzaka St, PL-01224 Warsaw, Poland.ORCID iD: 0000-0003-4457-2345
Polish Acad Sci, Inst Nucl Phys, 152 Radzikowskiego St, PL-31342 Krakow, Poland.ORCID iD: 0000-0001-7706-0296
Uppsala University, Disciplinary Domain of Science and Technology, Chemistry, Department of Chemistry - Ångström, Physical Chemistry. Polish Acad Sci, Inst Phys Chem, 44-52 Kasprzaka St, PL-01224 Warsaw, Poland.ORCID iD: 0000-0003-2124-9510
Polish Acad Sci, Inst Nucl Phys, 152 Radzikowskiego St, PL-31342 Krakow, Poland.ORCID iD: 0000-0002-7526-3097
2019 (English)In: Journal of Analytical Atomic Spectrometry, ISSN 0267-9477, E-ISSN 1364-5544, Vol. 34, no 7, p. 1409-1415Article in journal (Refereed) Published
Abstract [en]

X-ray spectroscopy studies are usually performed using synchrotron radiation sources, which offer bright, coherent, energy-tuneable and monochromatic light. However, the application of synchrotron-based Xray emission spectroscopy (XES) and X-ray absorption spectroscopy (XAS) is directly constrained by the limited, infrequent access to central facilities. With the advent of new technological solutions in the field of X-ray sources, optics and detectors, the development of efficient and compact laboratory X-ray spectroscopy systems is possible. A permanent laboratory-based setup offers the advantages of low cost and easy accessibility and, therefore, more flexibility in the preparation and scheduling of measurements. Herein, we report a laboratory X-ray setup allowing simultaneous XES and XAS measurements. The double von Hamos spectrometer performances are demonstrated by concurrent K beta XES and K-edge XAS measurements done for 3d elements.

Place, publisher, year, edition, pages
Royal Society of Chemistry, 2019. Vol. 34, no 7, p. 1409-1415
National Category
Atom and Molecular Physics and Optics
Identifiers
URN: urn:nbn:se:uu:diva-390902DOI: 10.1039/c9ja00159jISI: 000474289100021OAI: oai:DiVA.org:uu-390902DiVA, id: diva2:1343920
Available from: 2019-08-19 Created: 2019-08-19 Last updated: 2019-08-19Bibliographically approved

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Blachucki, WojciechCzapla-Masztafiak, JoannaSá, JacintoSzlachetko, Jakub
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