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Zirconium catalyzed amide formation without water scavenging
Umeå University, Faculty of Science and Technology, Department of Chemistry.ORCID iD: 0000-0001-5887-4630
2019 (English)In: Applied organometallic chemistry, ISSN 0268-2605, E-ISSN 1099-0739, Vol. 33, no 9, article id e5062Article in journal (Refereed) Published
Abstract [en]

A scalable homogeneous metal‐catalyzed protocol for direct amidation of carboxylic acids is presented. The use of 2–10 mol% of the commercially available Zr(Cp)2(OTf)2·THF results in high yields of amides at moderate temperature, using an operationally convenient reaction protocol that circumvents the use of water scavenging techniques.

Place, publisher, year, edition, pages
John Wiley & Sons, 2019. Vol. 33, no 9, article id e5062
Keywords [en]
mides, amines, carboxylic acids, catalysis, direct amidation, trifluoromethanesulfonate, zirconium
National Category
Organic Chemistry
Identifiers
URN: urn:nbn:se:umu:diva-161900DOI: 10.1002/aoc.5062ISI: 000476374900001Scopus ID: 2-s2.0-85069697551OAI: oai:DiVA.org:umu-161900DiVA, id: diva2:1341232
Funder
Knut and Alice Wallenberg FoundationSwedish Research CouncilAvailable from: 2019-08-08 Created: 2019-08-08 Last updated: 2020-01-09Bibliographically approved

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Lundberg, HelenaAdolfsson, Hans
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CiteExportLink to record
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Citation style
  • apa
  • ieee
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Output format
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