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One-Pot Synthesis of Unsymmetric Diaryliodonium Salts from Iodine and Arenes
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.
Stockholm University, Faculty of Science, Department of Organic Chemistry.ORCID iD: 0000-0001-7975-4582
2017 (English)In: Journal of Organic Chemistry, ISSN 0022-3263, E-ISSN 1520-6904, Vol. 82, no 22, p. 11909-11914Article in journal (Refereed) Published
Abstract [en]

The first synthesis of unsymmetric diaryliodonium salts directly from iodine and arenes is presented. The methodology provides diaryliodonium salts with the trimethoxyphenyl (TMP) moiety as dummy group. The protocol avoids the customary use of iodoarenes, which can be both expensive and toxic. Excess reagents are not required, and the reactions are performed under mild conditions. O-Arylations with these TMP salts were demonstrated to be highly chemoselective.

Place, publisher, year, edition, pages
2017. Vol. 82, no 22, p. 11909-11914
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:su:diva-149793DOI: 10.1021/acs.joc.7b01652ISI: 000416204400033PubMedID: 28809562OAI: oai:DiVA.org:su-149793DiVA, id: diva2:1167806
Funder
Swedish Research Council
Available from: 2017-12-19 Created: 2017-12-19 Last updated: 2018-02-19Bibliographically approved

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