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Facile synthesis of Koser's reagent and derivatives from iodine or aryl iodides
Stockholms universitet, Naturvetenskapliga fakulteten, Institutionen för organisk kemi.
Stockholms universitet, Naturvetenskapliga fakulteten, Institutionen för organisk kemi.
Stockholms universitet, Naturvetenskapliga fakulteten, Institutionen för organisk kemi.ORCID-id: 0000-0001-7975-4582
2010 (engelsk)Inngår i: Journal of Organic Chemistry, ISSN 0022-3263, E-ISSN 1520-6904, Vol. 75, nr 21, s. 7416-7419Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

The first one-pot synthesis of neutral and electron-rich [hydroxy(tosyloxy)iodo]arenes (HTIBs) from iodine and arenes is presented, thereby avoiding the need for expensive iodine(III) precursors. A large set of HTIBs, including a polyfluorinated analogue, can be obtained from the corresponding aryl iodide under the same conditions. The reaction proceeds under mild conditions, without excess reagents, and is fast and high-yielding. Together, the two presented routes give access to a wide range of HTIBs, which are useful reagents in a variety of synthetic transformations.

sted, utgiver, år, opplag, sider
2010. Vol. 75, nr 21, s. 7416-7419
HSV kategori
Forskningsprogram
organisk kemi
Identifikatorer
URN: urn:nbn:se:su:diva-54359DOI: 10.1021/jo101227jOAI: oai:DiVA.org:su-54359DiVA, id: diva2:393447
Forskningsfinansiär
Swedish Research Council, 621-2008-3709Knut and Alice Wallenberg Foundation
Tilgjengelig fra: 2011-01-31 Laget: 2011-01-31 Sist oppdatert: 2018-02-12bibliografisk kontrollert

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