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Direct, mild, and selective synthesis of unprotected dialdo-glycosides
KTH, Skolan för kemivetenskap (CHE), Kemi, Organisk kemi.
2006 (engelsk)Inngår i: European Journal of Organic Chemistry, ISSN 1434-193X, E-ISSN 1099-0690, nr 19, s. 4323-4326Artikkel i tidsskrift (Fagfellevurdert) Published
Abstract [en]

A direct and highly convenient organocatalytic method for the preparation of 1,5-dialdo-pyranosides and 1,4-dialdo-furanosides is presented. The method relies on the chemoselective properties of TEMPO in combination with trichloroisocyanuric acid under very mild, basic conditions. Unprotected glycosides are prepared in a single step in high yields and are efficiently purified with the use of solid-phase imine capture. ((c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2006).

sted, utgiver, år, opplag, sider
2006. nr 19, s. 4323-4326
Emneord [en]
glycosides, oxidation, catalysis, solid-phase, imine capture, catalyzed aerobic oxidation, galactose-oxidase, alcohols, sugar, scaffolds, recognition, aldehydes, glucose, design, acids
Identifikatorer
URN: urn:nbn:se:kth:diva-16049DOI: 10.1002/ejoc.200600288ISI: 000241204400002Scopus ID: 2-s2.0-33749448376OAI: oai:DiVA.org:kth-16049DiVA, id: diva2:334091
Merknad
QC 20100525Tilgjengelig fra: 2010-08-05 Laget: 2010-08-05 Sist oppdatert: 2017-12-12bibliografisk kontrollert

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